2R6U
Crystal structure of gene product RHA04853 from Rhodococcus sp. RHA1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-10-08 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97940 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 51.411, 89.048, 58.913 |
Unit cell angles | 90.00, 94.09, 90.00 |
Refinement procedure
Resolution | 58.720 - 1.500 |
R-factor | 0.17786 |
Rwork | 0.176 |
R-free | 0.21076 |
Structure solution method | SAD |
RMSD bond length | 0.013 |
RMSD bond angle | 1.550 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | HKL-3000 |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 58.720 | 1.538 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.072 | 0.343 |
Number of reflections | 79299 | |
<I/σ(I)> | 32.3 | 2.85 |
Completeness [%] | 98.7 | 88.54 |
Redundancy | 9.5 | 7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 298 | 0.1M Na(OAC), 0.2M Ammonium acetate, 30% PEG 4000, pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 298K |