2R6D
Crystal Form B1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 8.2.1 |
| Synchrotron site | ALS |
| Beamline | 8.2.1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2006-04-10 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 1.005 |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 371.260, 110.295, 112.606 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 20.000 - 3.700 |
| R-factor | 0.30966 |
| Rwork | 0.309 |
| R-free | 0.32228 |
| Structure solution method | MIR |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.416 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.2) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 3.830 |
| High resolution limit [Å] | 3.700 | 3.700 |
| Number of reflections | 92787 | |
| <I/σ(I)> | 15 | 1.8 |
| Completeness [%] | 97.3 | 86.6 |
| Redundancy | 3.7 | 3.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 5.5 | 298 | 1.0M Ammonium Acetate, pH 5.5, VAPOR DIFFUSION, temperature 298K |
