2QMZ

Quinone Reductase 2 in Complex with Dopamine

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 19-BM
Synchrotron site	APS
Beamline	19-BM
Temperature [K]	100
Detector technology	CCD
Collection date	2005-07-29
Detector	CUSTOM-MADE
Wavelength(s)	1
Spacegroup name	P 21 21 21
Unit cell lengths	83.442, 106.448, 56.533
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	50.000 - 2.100
Rwork	0.193
R-free	0.23800
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	CNS
Refinement software	CNS

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.100
Rmerge	0.101
Number of reflections	28148
<I/σ(I)>	15
Completeness [%]	93.6
Redundancy	6.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7	300	Ammonium Sulfate (1.2-2 M), pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 300K