2QLW
Crystal structure of rhamnose mutarotase RhaU of Rhizobium leguminosarum
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM16 |
Synchrotron site | ESRF |
Beamline | BM16 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-02-23 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.9079 |
Spacegroup name | P 32 1 2 |
Unit cell lengths | 69.241, 69.241, 101.106 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.990 - 1.600 |
R-factor | 0.153 |
Rwork | 0.152 |
R-free | 0.18000 |
Structure solution method | SAD |
RMSD bond length | 0.018 |
RMSD bond angle | 1.690 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHELX |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.660 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.097 | 0.589 |
Number of reflections | 35978 | |
<I/σ(I)> | 11.2 | 3.2 |
Completeness [%] | 97.1 | 97 |
Redundancy | 5.7 | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 298 | 2M Sodium Formate, 0.1M Sodium Acetate pH 4.6, 20% Glycerol , VAPOR DIFFUSION, HANGING DROP, temperature 298K |