2QEN
The walker-type atpase paby2304 of pyrococcus abyssi
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-09-09 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.2836,0.849972 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 80.614, 49.195, 108.863 |
Unit cell angles | 90.00, 98.10, 90.00 |
Refinement procedure
Resolution | 28.300 - 2.250 |
R-factor | 0.199 |
Rwork | 0.197 |
R-free | 0.24800 |
Structure solution method | MAD |
RMSD bond length | 0.011 |
RMSD bond angle | 1.314 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.300 | 2.300 |
High resolution limit [Å] | 2.250 | 2.250 |
Rmerge | 0.043 | 0.120 |
Number of reflections | 18280 | |
Completeness [%] | 95.0 | 91.6 |
Redundancy | 3.1 | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 20% PEG 3350, PH 6.5, VAPOR DIFFUSION, SITTING DROP, TEMPERATURE 297K, pH 6.50 |