2QB6
Saccharomyces cerevisiae cytosolic exopolyphosphatase, sulfate complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.93400 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 79.660, 82.914, 119.228 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.400 - 1.800 |
R-factor | 0.15944 |
Rwork | 0.157 |
R-free | 0.20099 |
Structure solution method | MIR |
RMSD bond length | 0.014 |
RMSD bond angle | 1.467 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.400 | 1.890 |
High resolution limit [Å] | 1.800 | 1.800 |
Number of reflections | 64994 | |
<I/σ(I)> | 8.5 | 3.7 |
Completeness [%] | 88.2 | 51.4 |
Redundancy | 4.3 | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 291 | 7% PEG 4000, 150 mM (NH4)2SO4, pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 291K |