2PIN

Thyroid receptor beta in complex with inhibitor

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 8.3.1
Synchrotron site	ALS
Beamline	8.3.1
Temperature [K]	100
Detector technology	CCD
Collection date	2005-11-02
Detector	ADSC QUANTUM 210
Spacegroup name	P 1 21 1
Unit cell lengths	55.130, 92.870, 58.350
Unit cell angles	90.00, 109.65, 90.00

Refinement procedure

Resolution	25.000 - 2.300
Rwork	0.216
R-free	0.25600
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	ELVES
Data scaling software	SCALA
Phasing software	CNS
Refinement software	ELVES

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	25.000
High resolution limit [Å]	2.300	2.300
Number of reflections	24674

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	VAPOR DIFFUSION, HANGING DROP, temperature 298K