Experimental procedure
| Collection date | 1991-11-01 |
| Spacegroup name | P 63 |
| Unit cell lengths | 66.900, 66.900, 40.800 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 20.000 - 1.400 |
| R-factor | 0.186 |
| Rwork | 0.186 |
| R-free | 0.22600 |
| RMSD bond length | 0.012 |
| RMSD bond angle | 25.400 * |
| Data reduction software | XENGEN |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 9999.000 * | |
| High resolution limit [Å] | 1.400 | 1.400 * |
| Rmerge | 0.040 | 0.207 * |
| Number of reflections | 19756 | 3449 * |
| Completeness [%] | 92.7 | |
| Redundancy | 3.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 7 * | used as seeds * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | 3.2 (M) | ||
| 2 | 1 | reservoir | sodium phosphate | 20 (mM) | |
| 3 | 1 | drop | protein | 15 (mg/ml) | |
| 4 | 1 | drop | 2.5 (M) | ||
| 5 | 1 | drop | sodium phosphate | 20 (mM) |
