Experimental procedure
Detector technology | AREA DETECTOR |
Collection date | 1996-01 |
Detector | SIEMENS |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 156.230, 49.040, 42.250 |
Unit cell angles | 90.00, 98.60, 90.00 |
Refinement procedure
Resolution | 9.000 - 2.000 * |
R-factor | 0.186 * |
RMSD bond length | 0.009 |
RMSD bond angle | 18.000 * |
Data reduction software | SAINT |
Refinement software | TNT |
Data quality characteristics
Overall | |
Rmerge | 0.052 |
Total number of observations | 46251 * |
Number of reflections | 19026 |
Completeness [%] | 85.5 |
Redundancy | 2.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, sitting drop * | 7.4 * | 20 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | ammonium salfate | 1.8-1.9 (M) | |
2 | 1 | reservoir | sodium phosphate | 30 (mM) |