Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL9-2 |
| Synchrotron site | SSRL |
| Beamline | BL9-2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.9788, 0.9791, 0.9184, 1.009 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 184.274, 184.274, 260.485 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 50.000 - 3.700 |
| Rwork | 0.293 |
| R-free | 0.32100 |
| Structure solution method | MAD |
| Starting model (for MR) | 1MXM |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.636 |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 3.810 |
| High resolution limit [Å] | 3.700 | 3.700 |
| Rmerge | 0.956 | |
| Number of reflections | 48452 | |
| <I/σ(I)> | 20.7 | 2 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 8.1 | 7.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.2 | 277 | PEG 3350, AMMONIUM CHLORIDE, CITRATE, FOSHOLINE-14, pH 7.2, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
