2JJZ

Crystal Structure of Human Iba2, orthorhombic crystal form

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	BESSY BEAMLINE 14.1
Synchrotron site	BESSY
Beamline	14.1
Temperature [K]	100
Detector technology	CCD
Detector	MARRESEARCH
Spacegroup name	P 21 21 2
Unit cell lengths	71.540, 186.500, 51.420
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.810 - 2.150
R-factor	0.218
Rwork	0.216
R-free	0.25700
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1wy9
RMSD bond length	0.018
RMSD bond angle	1.588
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	REFMAC (5.3.0040)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000	2.250
High resolution limit [Å]	2.150	2.150
Rmerge	0.080	0.750
Number of reflections	38251
<I/σ(I)>	16.1	3
Completeness [%]	99.7	100
Redundancy	7.3	7.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1