2JH0

Human Thrombin Hirugen Inhibitor complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU200
Temperature [K]	100
Detector technology	CCD
Collection date	2002-09-24
Detector	RIGAKU CCD
Spacegroup name	C 1 2 1
Unit cell lengths	70.070, 71.556, 71.931
Unit cell angles	90.00, 100.12, 90.00

Refinement procedure

Resolution	20.000 - 1.700
R-factor	0.184
Rwork	0.183
R-free	0.21000
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.010
RMSD bond angle	1.553
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	REFMAC (5.3.0006)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000	1.760
High resolution limit [Å]	1.700	1.700
Rmerge	0.040	0.370
Number of reflections	35898
Completeness [%]	99.8
Redundancy	3.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		6.8		PH 6.80