2JGR
Crystal structure of YegS in complex with ADP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-3 |
| Synchrotron site | ESRF |
| Beamline | ID14-3 |
| Temperature [K] | 287 |
| Detector technology | CCD |
| Collection date | 2005-04-23 |
| Detector | MARRESEARCH |
| Spacegroup name | P 42 21 2 |
| Unit cell lengths | 124.968, 124.968, 54.163 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 88.390 - 2.650 |
| R-factor | 0.205 |
| Rwork | 0.203 |
| R-free | 0.24900 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2bon |
| RMSD bond length | 0.022 |
| RMSD bond angle | 2.072 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 88.000 |
| High resolution limit [Å] | 2.650 |
| Rmerge | 0.090 |
| Number of reflections | 11841 |
| <I/σ(I)> | 12 |
| Completeness [%] | 97.1 |
| Redundancy | 4.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
