2JDA
Structure of a pectin binding carbohydrate binding module determined in an monoclinic crystal form.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 113 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 111.205, 34.729, 86.711 |
| Unit cell angles | 90.00, 120.58, 90.00 |
Refinement procedure
| Resolution | 20.000 - 1.350 |
| R-factor | 0.145 |
| Rwork | 0.143 |
| R-free | 0.18000 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.019 |
| RMSD bond angle | 1.924 |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 1.400 |
| High resolution limit [Å] | 1.350 | 1.350 |
| Rmerge | 0.030 | 0.260 |
| Number of reflections | 56372 | |
| <I/σ(I)> | 22.3 | 2 |
| Completeness [%] | 89.3 | 38.6 |
| Redundancy | 3.7 | 1.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
