2J8W
The crystal structure of cytochrome c' from Rubrivivax gelatinosus at 1.3 A Resolution and pH 8.0
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE BW7B |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | BW7B |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1996-10-10 |
Detector | MARRESEARCH |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 69.630, 69.630, 123.630 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.960 - 1.290 |
R-factor | 0.151 |
Rwork | 0.151 |
R-free | 0.17900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1jaf |
RMSD bond length | 0.016 |
RMSD bond angle | 1.744 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.940 | 1.310 |
High resolution limit [Å] | 1.290 | 1.290 |
Rmerge | 0.040 | 0.380 |
Number of reflections | 87744 | |
<I/σ(I)> | 33.7 | 3.58 |
Completeness [%] | 99.8 | 99.3 |
Redundancy | 5.1 | 3.48 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | HANGING DROP 2.5 M AMMONIUM SULPHATE 0.1M TRIS-HCL PH8.0 |