2J88
Hyaluronidase in complex with a monoclonal IgG Fab fragment
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-11-24 |
Detector | MARRESEARCH |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 151.563, 70.050, 138.880 |
Unit cell angles | 90.00, 123.68, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 63.630 | 2.740 |
High resolution limit [Å] | 2.500 | 2.600 |
Rmerge | 0.080 | 0.300 |
Number of reflections | 32047 | |
<I/σ(I)> | 6.98 | 2.15 |
Completeness [%] | 85.4 | 81.8 |
Redundancy | 3.17 | 3.19 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 9.5 | 10% PEG 8000, 0.2M NACL, 0.1M CHES PH9.5, pH 9.50 |