2J58
The structure of Wza
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-11-19 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 94.719, 215.268, 220.892 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 107.830 - 2.250 |
R-factor | 0.19 |
Rwork | 0.188 |
R-free | 0.22600 |
Structure solution method | SAD |
RMSD bond length | 0.012 |
RMSD bond angle | 1.292 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHELX |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 108.000 | 2.320 |
High resolution limit [Å] | 2.260 | 2.260 |
Rmerge | 0.080 | 0.350 |
Number of reflections | 200359 | |
<I/σ(I)> | 18.4 | 1.8 |
Completeness [%] | 99.0 | 94.9 |
Redundancy | 5 | 2.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |