2J2P

L-ficolin complexed to N-acetyl-cystein (150mM)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-2
Synchrotron site	ESRF
Beamline	ID14-2
Temperature [K]	100
Detector technology	CCD
Collection date	2006-02-11
Detector	ADSC CCD
Spacegroup name	P 32
Unit cell lengths	96.400, 96.400, 140.290
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	19.970 - 2.800
R-factor	0.201
Rwork	0.197
R-free	0.27000
Structure solution method	OTHER
RMSD bond length	0.008
RMSD bond angle	1.098
Data reduction software	XDS
Data scaling software	XSCALE
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	19.970
High resolution limit [Å]	2.800
Rmerge	0.130
Number of reflections	33431
<I/σ(I)>	6.3
Completeness [%]	90.9
Redundancy	2.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1