2J1S
Structure of a Streptococcus pneumoniae fucose binding module in complex with fucose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 113 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.523, 60.771, 99.499 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.500 |
R-factor | 0.157 |
Rwork | 0.155 |
R-free | 0.19200 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.017 |
RMSD bond angle | 1.640 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.550 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.040 | 0.250 |
Number of reflections | 38029 | |
<I/σ(I)> | 19.3 | 2.9 |
Completeness [%] | 93.1 | 54.9 |
Redundancy | 4 | 1.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |