2IYN

The co-factor-induced pre-active conformation in PhoB

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	EMBL/DESY, HAMBURG BEAMLINE BW7A
Synchrotron site	EMBL/DESY, HAMBURG
Beamline	BW7A
Temperature [K]	100
Detector technology	CCD
Detector	MARRESEARCH
Spacegroup name	C 2 2 21
Unit cell lengths	50.742, 105.829, 135.510
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	50.000 - 2.080
R-factor	0.233
Rwork	0.231
R-free	0.30500
Structure solution method	OTHER
RMSD bond length	0.016
RMSD bond angle	1.503
Refinement software	REFMAC (5.1.24)

Data quality characteristics

	Overall
Low resolution limit [Å]	45.200
High resolution limit [Å]	2.080
Rmerge	0.080
Number of reflections	20372
<I/σ(I)>	5.2
Completeness [%]	91.4
Redundancy	5.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1