2IPP
Crystal Structure of the tetragonal form of human liver cathepsin B
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 271 |
Detector technology | AREA DETECTOR |
Collection date | 1989-07-31 |
Detector | ADSC |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 |
Unit cell lengths | 85.580, 85.580, 34.390 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.150 |
R-factor | 0.157 |
Structure solution method | MOLECULAR REPLACEMENT |
Phasing software | X-PLOR |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 19.500 |
High resolution limit [Å] | 2.000 |
Rmerge | 0.102 |
Number of reflections | 13463 |
Completeness [%] | 99.3 |
Redundancy | 5.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4 | 293 | pH 4.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |