2ICK

Human isopentenyl diphophate isomerase complexed with substrate analog

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU
Temperature [K]	100
Detector technology	AREA DETECTOR
Collection date	2005-12-05
Detector	MARRESEARCH
Wavelength(s)	1.5418
Spacegroup name	P 21 21 21
Unit cell lengths	40.812, 47.396, 116.817
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	50.000 - 1.930
R-factor	0.214
Rwork	0.205
R-free	0.25500
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2icj
RMSD bond length	0.012
RMSD bond angle	1.764
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	CNS
Refinement software	CNS

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.000
High resolution limit [Å]	1.930	1.930
Number of reflections	17807
Completeness [%]	93.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1