2I7P
Crystal structure of human PANK3 in complex with AcCoA
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-BM |
| Synchrotron site | APS |
| Beamline | 19-BM |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2006-02-25 |
| Detector | SBC-3 |
| Wavelength(s) | 0.9 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 56.734, 180.170, 77.728 |
| Unit cell angles | 90.00, 95.68, 90.00 |
Refinement procedure
| Resolution | 29.340 - 2.050 |
| R-factor | 0.211 |
| Rwork | 0.211 |
| R-free | 0.25300 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.200 |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 2.120 |
| High resolution limit [Å] | 2.050 | 2.050 |
| Rmerge | 0.061 | 0.446 |
| Number of reflections | 96048 | |
| <I/σ(I)> | 13.3 | 1.27 |
| Completeness [%] | 98.8 | 90.5 |
| Redundancy | 3.5 | 2.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 298 | 1M Tris, 50% PEG3350, 2M NH4Citrate, pH 8.5, VAPOR DIFFUSION, SITTING DROP, temperature 298K |
