2HQH
Crystal structure of p150Glued and CLIP-170
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-BM |
| Synchrotron site | APS |
| Beamline | 19-BM |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-06-05 |
| Detector | CUSTOM-MADE |
| Wavelength(s) | 0.9791, 1.2826, 1.2830, 1.2694 |
| Spacegroup name | P 42 21 2 |
| Unit cell lengths | 122.800, 122.800, 68.400 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 45.680 - 1.800 |
| Rwork | 0.194 |
| R-free | 0.21550 |
| Structure solution method | MAD |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SnB |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 45.700 | 1.860 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Number of reflections | 49011 | |
| Completeness [%] | 100.0 | 100 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7 | 298 | 4M sodium formate, pH 7, VAPOR DIFFUSION, SITTING DROP, temperature 298K |
