2HE7
FERM domain of EPB41L3 (DAL-1)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-05-22 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.07 |
Spacegroup name | P 65 |
Unit cell lengths | 135.500, 135.500, 49.800 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.340 - 2.000 |
R-factor | 0.188 |
Rwork | 0.187 |
R-free | 0.21700 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.021 |
RMSD bond angle | 1.735 |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.100 | |
High resolution limit [Å] | 2.000 | 6.000 | 2.000 |
Rmerge | 0.025 | 0.561 | |
Number of reflections | 35521 | ||
<I/σ(I)> | 21.13 | 70.1 | 4.8 |
Completeness [%] | 99.4 | 100 | 98.4 |
Redundancy | 11 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293 | 20% EtOH 0.1 M Tris pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |