2H4L
Complex of PMM/PGM with ribose 1-phosphate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 14-BM-C |
Synchrotron site | APS |
Beamline | 14-BM-C |
Temperature [K] | 100 |
Wavelength(s) | 1.0398 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 70.717, 74.095, 84.347 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.850 - 2.400 |
R-factor | 0.18998 |
Rwork | 0.186 |
R-free | 0.25946 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 1p5d |
RMSD bond length | 0.009 |
RMSD bond angle | 1.192 |
Data scaling software | HKL-2000 |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Number of reflections | 16595 | |
Completeness [%] | 91.7 | 83.9 |
Redundancy | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | NA, K TARTRATE , pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |