2H1C
Crystal Structure of FitAcB from Neisseria gonorrhoeae
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.1 |
Synchrotron site | ALS |
Beamline | 8.2.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-03-08 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.0000 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 69.970, 50.700, 48.280 |
Unit cell angles | 90.00, 118.55, 90.00 |
Refinement procedure
Resolution | 39.110 - 1.800 |
R-factor | 0.223 |
Rwork | 0.191 |
R-free | 0.22300 |
Structure solution method | MAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.300 |
Data reduction software | MOSFLM |
Phasing software | SOLVE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.110 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Number of reflections | 13340 | |
<I/σ(I)> | 3.1 | |
Completeness [%] | 96.5 | 95.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.7 | 298 | 0.26 M sodium phosphate/citrate pH 4.7 and 2.0 M ammonium sulphate, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
1 | VAPOR DIFFUSION, HANGING DROP | 4.7 | 298 | 0.26 M sodium phosphate/citrate pH 4.7 and 2.0 M ammonium sulphate, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
1 | VAPOR DIFFUSION, HANGING DROP | 4.7 | 298 | 0.26 M sodium phosphate/citrate pH 4.7 and 2.0 M ammonium sulphate, VAPOR DIFFUSION, HANGING DROP, temperature 298K |