Experimental procedure
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 76.080, 27.780, 42.000 |
| Unit cell angles | 90.00, 102.70, 90.00 |
Refinement procedure
| Resolution | ? - 2.300 |
| R-factor | 0.217 * |
| Rwork | 0.217 |
| RMSD bond length | 0.040 |
| RMSD bond angle | 0.176 |
| Refinement software | PROLSQ |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.300 * |
| Total number of observations | 8747 * |
| Number of reflections | 3905 * |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion * | 7.6 * | referred to J.Mol.Biol. 106.1077-1081 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | protein | 15 (mg/ml) | |
| 2 | 1 | drop | Tris-HCl | 0.05 (M) | |
| 3 | 1 | drop | PEG4000 | 20 (%) | |
| 4 | 1 | reservoir | PEG4000 | 10 (%) |
