2GEL

2.05A crystal structure of Salmonella typhimurium YeaZ, form B

Experimental procedure

Experimental method	MAD
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-2
Synchrotron site	ESRF
Beamline	ID14-2
Temperature [K]	100
Detector technology	CCD
Collection date	2005-09-20
Detector	ADSC QUANTUM 4
Wavelength(s)	0.93300
Spacegroup name	P 21 21 2
Unit cell lengths	144.199, 83.658, 41.260
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.000 - 2.050
R-factor	0.22
Rwork	0.195
R-free	0.22700
Structure solution method	MAD
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	CNS
Refinement software	CNS

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000	2.100
High resolution limit [Å]	2.050	2.050
Number of reflections	29954
Completeness [%]	94.0	84

Crystallization Conditions

crystal ID	method	pH	temperature	details
1