2G88
MSRECA-dATP COMPLEX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 293 |
Detector technology | IMAGE PLATE |
Collection date | 2004-01-05 |
Detector | MARRESEARCH |
Spacegroup name | P 61 |
Unit cell lengths | 108.212, 108.212, 72.970 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 25.400 - 3.200 |
R-factor | 0.237 |
Rwork | 0.237 |
R-free | 0.30900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ubc |
RMSD bond length | 0.014 |
RMSD bond angle | 2.800 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (0.4) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.400 | 3.310 |
High resolution limit [Å] | 3.200 | 3.200 |
Rmerge | 0.103 | 0.530 |
Number of reflections | 7941 | |
<I/σ(I)> | 6.3 | 1.7 |
Completeness [%] | 97.5 | 100 |
Redundancy | 4.1 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 0.1M citrate phosphate, 30% 4000 PEG, 0.1M sodium citrate, 10% glycerol, 0.1M Nacl, 0.2M ammonium acetate, 0.025 DTT, 0.025 sodium azide, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |