2FWR
Structure of Archaeoglobus Fulgidis XPB
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 5.0.2 |
| Synchrotron site | ALS |
| Beamline | 5.0.2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2001-10-27 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 |
| Unit cell lengths | 49.085, 97.963, 113.731 |
| Unit cell angles | 79.03, 85.54, 89.69 |
Refinement procedure
| Resolution | 29.350 - 2.600 |
| R-factor | 0.221 |
| Rwork | 0.237 |
| R-free | 0.30000 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.500 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 2.690 |
| High resolution limit [Å] | 2.600 | 2.600 |
| Rmerge | 0.094 | 0.405 |
| Number of reflections | 57207 | 3271 |
| <I/σ(I)> | 9.9 | |
| Completeness [%] | 88.9 | 51.1 |
| Redundancy | 2.4 | 1.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | TRIS/HCL, PEG 20K, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
