2FSG
Complex SecA:ATP from Escherichia coli
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.97889 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 75.382, 89.478, 163.349 |
Unit cell angles | 90.00, 100.73, 90.00 |
Refinement procedure
Resolution | 19.610 - 2.200 |
Rwork | 0.208 |
R-free | 0.27000 |
Structure solution method | SAD |
RMSD bond length | 0.034 |
RMSD bond angle | 2.400 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHELXD |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 20.000 | 59.740 | 2.320 |
High resolution limit [Å] | 2.200 | 6.960 | 2.200 |
Rmerge | 0.077 | 0.020 | 0.644 |
Total number of observations | 13042 | 49535 | |
Number of reflections | 106818 | 3539 | 14458 |
<I/σ(I)> | 8.5 | 29.7 | 1.1 |
Completeness [%] | 96.9 | 99.5 | 92 |
Redundancy | 3.5 | 3.7 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |