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2FJS

Crystal Structure of Anaerobically Reduced Wild Type Nitrite Reductase from A. faecalis

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RU300
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2005-04-15
DetectorMARRESEARCH
Wavelength(s)1.5418
Spacegroup nameP 21 21 21
Unit cell lengths61.552, 102.428, 145.744
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution30.000 - 1.850
R-factor0.15192
Rwork0.150
R-free0.18040
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1snr
RMSD bond length0.010
RMSD bond angle1.264
Data scaling softwareSCALEPACK
Phasing softwareAMoRE
Refinement softwareREFMAC (5.2.0005)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0001.920
High resolution limit [Å]1.8501.850
Rmerge0.1160.410
Number of reflections72738
Completeness [%]91.5100
Redundancy4.35
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP42988-10% PEG 4000, 0.1 M NaOAC, pH 4, VAPOR DIFFUSION, HANGING DROP, temperature 298K

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