2FA1
Crystal structure of PhnF C-terminal domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-BM |
Synchrotron site | APS |
Beamline | 19-BM |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-10-10 |
Detector | CUSTOM-MADE |
Wavelength(s) | 0.97944 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 46.765, 51.572, 63.961 |
Unit cell angles | 90.00, 103.64, 90.00 |
Refinement procedure
Resolution | 50.000 - 1.700 |
R-factor | 0.18958 |
Rwork | 0.187 |
R-free | 0.24121 |
Structure solution method | SAD |
RMSD bond length | 0.025 |
RMSD bond angle | 2.332 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.760 |
High resolution limit [Å] | 1.700 | 1.700 |
Number of reflections | 32745 | |
<I/σ(I)> | 33.1 | 2.75 |
Completeness [%] | 99.9 | 99.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 297 | 20% PEG3350, 0.2M Mg Formate, 50mMtris pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 297K |