2F38
Crystal structure of prostaglandin F synathase containing bimatoprost
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 95 |
Detector technology | IMAGE PLATE |
Collection date | 2005-05-05 |
Detector | RIGAKU RAXIS IIC |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 44.270, 78.160, 48.890 |
Unit cell angles | 90.00, 100.20, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.000 |
R-factor | 0.221 |
Rwork | 0.220 |
R-free | 0.28100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ry0 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR |
Refinement software | X-PLOR (98.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.100 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 19525 | |
Completeness [%] | 89.0 | 63 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 277 | 1.0 mM BMP, 1.0 mM NADPH, 0.14 M NaCl, 50 mM MES, 26% PEG-8000, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K |