2E12
The crystal structure of XC5848 from Xanthomonas campestris adopting a novel variant of Sm-like motif
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | NSRRC BEAMLINE BL13B1 |
| Synchrotron site | NSRRC |
| Beamline | BL13B1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2006-07-28 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.96437, 0.97983 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 49.942, 51.699, 82.120 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 30.000 - 1.700 |
| R-factor | 0.24 |
| Rwork | 0.220 |
| R-free | 0.28000 |
| Structure solution method | MAD |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.315 |
| Data reduction software | DENZO |
| Data scaling software | HKL-2000 |
| Phasing software | AMoRE |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | |
| High resolution limit [Å] | 1.700 | 1.700 |
| Rmerge | 0.240 | 0.240 |
| Number of reflections | 6937 | |
| <I/σ(I)> | 8 | 7.9 |
| Completeness [%] | 99.7 | 97.5 |
| Redundancy | 4.5 | 4.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8 | 298 | pH 8.0, VAPOR DIFFUSION, SITTING DROP, temperature 298K |
