2DES
INTERACTIONS BETWEEN MORPHOLINYL ANTHRACYCLINES AND DNA: THE CRYSTAL STRUCTURE OF A MORPHOLINO DOXORUBICIN BOUND TO D(CGTACG)
Experimental procedure
| Detector technology | DIFFRACTOMETER |
| Detector | SYNTEX P21 |
| Spacegroup name | P 1 |
| Unit cell lengths | 18.010, 18.830, 26.750 |
| Unit cell angles | 92.60, 100.50, 94.90 |
Refinement procedure
| Resolution | 10.000 - 1.500 |
| R-factor | 0.192 |
| Refinement software | NUCLSQ |
Data quality characteristics
| Overall | |
| Number of reflections | 3988 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | other * | 5.5 | pH 5.50, VAPOR DIFFUSION, SITTING DROP |
Crystallization Reagents
| ID | crystal ID | solution ID | reagent name | concentration | details |
| 1 | 1 | 1 | WATER | ||
| 2 | 1 | 1 | MPD | ||
| 3 | 1 | 1 | NA CACODYLATE | ||
| 4 | 1 | 1 | MGCL2 | ||
| 5 | 1 | 1 | SPERMINE_HCL | ||
| 6 | 1 | 2 | WATER | ||
| 7 | 1 | 2 | MPD |
