2CW2
Crystal structure of Superoxide dismutase from P. Marinus
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Detector | MARRESEARCH |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 53.813, 62.451, 57.354 |
| Unit cell angles | 90.00, 95.54, 90.00 |
Refinement procedure
| Resolution | 56.800 - 1.860 |
| R-factor | 0.17309 |
| Rwork | 0.171 |
| R-free | 0.21560 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.313 |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 56.800 | 1.930 |
| High resolution limit [Å] | 1.860 | 1.860 |
| Rmerge | 0.046 | 0.295 |
| Number of reflections | 32044 | |
| Completeness [%] | 95.0 | 91 |
| Redundancy | 5.5 | 4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | VAPOR DIFFUSION, HANGING DROP |
