2CVD
Crystal structure analysis of human hematopoietic prostaglandin D synthase complexed with HQL-79
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL41XU |
| Synchrotron site | SPring-8 |
| Beamline | BL41XU |
| Detector technology | CCD |
| Collection date | 2001-04-24 |
| Detector | MARRESEARCH |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 |
| Unit cell lengths | 46.937, 49.085, 93.137 |
| Unit cell angles | 85.83, 88.71, 89.98 |
Refinement procedure
| Resolution | 34.980 - 1.450 |
| R-factor | 0.192 |
| Rwork | 0.192 |
| R-free | 0.20900 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1iyh |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.400 |
| Refinement software | CNS (1.0) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 100.000 |
| High resolution limit [Å] | 1.450 |
| Number of reflections | 1287104 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
