Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | LURE BEAMLINE DW32 |
Synchrotron site | LURE |
Beamline | DW32 |
Temperature [K] | 300 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 35.660, 73.420, 91.320 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 57.260 - 2.130 |
R-factor | 0.169 |
Rwork | 0.167 |
R-free | 0.22400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1bsg |
RMSD bond length | 0.020 |
RMSD bond angle | 1.923 |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 57.260 | 2.180 |
High resolution limit [Å] | 2.130 | 2.130 |
Rmerge | 0.060 | |
Number of reflections | 11576 | |
Completeness [%] | 86.9 | 53 |
Redundancy | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |