2CBN

Crystal structure of ZipD from Escherichia coli

Experimental procedure

Experimental method	MAD
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	CCD
Detector	MARRESEARCH
Spacegroup name	P 64 2 2
Unit cell lengths	147.200, 147.200, 138.200
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	50.000 - 2.900
R-factor	0.23
Rwork	0.230
R-free	0.25000
Structure solution method	MAD
RMSD bond length	0.010
RMSD bond angle	1.600
Data reduction software	XDS
Data scaling software	XDS
Phasing software	XPREP
Refinement software	CNS (1.0)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.900
Rmerge	0.070
Number of reflections	20073
Completeness [%]	100.0
Redundancy	15

Crystallization Conditions

crystal ID	method	pH	temperature	details
1