2CB0

Crystal structure of glucosamine 6-phosphate deaminase from Pyrococcus furiosus

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 4A
Synchrotron site	PAL/PLS
Beamline	4A
Temperature [K]	100
Detector technology	CCD
Collection date	2005-12-02
Detector	ADSC CCD
Spacegroup name	C 2 2 21
Unit cell lengths	61.480, 93.890, 200.650
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	28.040 - 1.800
R-factor	0.172
Rwork	0.170
R-free	0.21900
Structure solution method	OTHER
RMSD bond length	0.016
RMSD bond angle	1.498
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Refinement software	REFMAC (5.2.0005)

Data quality characteristics

	Overall
Low resolution limit [Å]	30.000
High resolution limit [Å]	1.800
Rmerge	0.080
Number of reflections	40401
Completeness [%]	74.0
Redundancy	5.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		6		pH 6.00