2C6R
FE-SOAKED CRYSTAL STRUCTURE OF THE DPS92 FROM DEINOCOCCUS RADIODURANS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-07-13 |
Detector | ADSC CCD |
Wavelength(s) | 1.1070,1.7399 |
Spacegroup name | P 2 3 |
Unit cell lengths | 88.965, 88.965, 88.965 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 89.090 - 2.100 |
R-factor | 0.188 |
Rwork | 0.188 |
Structure solution method | SAD |
RMSD bond length | 0.016 |
RMSD bond angle | 1.422 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.660 | 2.050 |
High resolution limit [Å] | 2.100 | 2.000 |
Rmerge | 0.090 | 0.850 |
Number of reflections | 13986 | |
<I/σ(I)> | 16.9 | 1.7 |
Completeness [%] | 99.9 | 100 |
Redundancy | 7.3 | 7.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 0.01M MGCL2, 0.05M TRIS PH7.5, 5% ISOPROPANOL, pH 7.50 |