2C03
GDP COMPLEX OF SRP GTPASE FFH NG DOMAIN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 5ID-B |
Synchrotron site | APS |
Beamline | 5ID-B |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 1998-09-14 |
Detector | MARRESEARCH |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 108.590, 55.110, 96.110 |
Unit cell angles | 90.00, 101.73, 90.00 |
Refinement procedure
Resolution | 19.960 - 1.240 |
R-factor | 0.138 |
Rwork | 0.134 |
R-free | 0.18400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ffh |
RMSD bond length | 0.010 |
RMSD bond angle | 1.396 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.270 |
High resolution limit [Å] | 1.240 | 1.240 |
Rmerge | 0.063 | 0.470 |
Number of reflections | 154602 | |
<I/σ(I)> | 12.5 | 2 |
Completeness [%] | 94.6 | 96.1 |
Redundancy | 3.6 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 30% DIOXANE, 2MM GDP |