2BXB
Human serum albumin complexed with oxyphenbutazone
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SRS BEAMLINE PX9.6 |
| Synchrotron site | SRS |
| Beamline | PX9.6 |
| Temperature [K] | 298 |
| Detector technology | CCD |
| Collection date | 2002-10-15 |
| Detector | ADSC CCD |
| Spacegroup name | P 1 |
| Unit cell lengths | 55.160, 55.500, 120.510 |
| Unit cell angles | 81.33, 90.52, 65.38 |
Refinement procedure
| Resolution | 22.880 - 3.200 |
| R-factor | 0.228 |
| Rwork | 0.228 |
| R-free | 0.27600 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1e78 |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.200 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | CNS |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 22.900 | 3.370 |
| High resolution limit [Å] | 3.200 | 3.200 |
| Rmerge | 0.070 | 0.340 |
| Number of reflections | 22484 | |
| <I/σ(I)> | 8 | 2.5 |
| Completeness [%] | 96.8 | 97 |
| Redundancy | 1.8 | 1.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | pH 7.00 |
