2BX8

Human serum albumin complexed with azapropazone

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	EMBL/DESY, HAMBURG BEAMLINE X11
Synchrotron site	EMBL/DESY, HAMBURG
Beamline	X11
Temperature [K]	298
Detector technology	CCD
Collection date	2004-02-15
Detector	MARRESEARCH
Spacegroup name	P 1
Unit cell lengths	54.200, 54.950, 119.903
Unit cell angles	81.21, 91.07, 64.75

Refinement procedure

Resolution	41.450 - 2.700
R-factor	0.237
Rwork	0.237
R-free	0.27300
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1e78
RMSD bond length	0.009
RMSD bond angle	1.400
Data reduction software	MOSFLM
Data scaling software	SCALA
Phasing software	CNS
Refinement software	CNS (1.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	41.500	2.850
High resolution limit [Å]	2.700	2.700
Rmerge	0.040	0.300
Number of reflections	32332
<I/σ(I)>	12.2	2.9
Completeness [%]	95.6	95.4
Redundancy	2	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		7		pH 7.00