2BWK
Murine angiogenin, sulphate complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX9.6 |
Synchrotron site | SRS |
Beamline | PX9.6 |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 1999-09-20 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 63.762, 56.266, 35.343 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.180 - 1.500 |
R-factor | 0.179 |
Rwork | 0.178 |
R-free | 0.19100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1agi |
RMSD bond length | 0.015 |
RMSD bond angle | 1.616 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0003) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.550 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.070 | 0.220 |
Number of reflections | 20302 | |
<I/σ(I)> | 17 | 5 |
Completeness [%] | 96.3 | 83.4 |
Redundancy | 6.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.5 | 25% PEG 4000, 0.2M (NH4)2SO4, UNBUFFERED, pH 4.50 |