2BQ4
Crystal structure of type I cytochrome c3 from Desulfovibrio africanus
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-2 |
| Synchrotron site | ESRF |
| Beamline | ID14-2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-01-31 |
| Detector | MARRESEARCH |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 100.900, 46.300, 54.816 |
| Unit cell angles | 90.00, 118.97, 90.00 |
Refinement procedure
| Resolution | 48.220 - 1.680 |
| R-factor | 0.202 |
| Rwork | 0.200 |
| R-free | 0.24000 |
| Structure solution method | SAD |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.379 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | SHARP |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.220 | 1.750 |
| High resolution limit [Å] | 1.680 | 1.680 |
| Rmerge | 0.060 | 0.060 |
| Number of reflections | 106337 | |
| <I/σ(I)> | 20.2 | 11.3 |
| Completeness [%] | 94.8 | 71.8 |
| Redundancy | 3.9 | 2.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 3.2M NAH2PO4/K2HPO4 |
