2BOK
Factor Xa - cation
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | ENRAF-NONIUS FR591 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2004-12-14 |
| Detector | MARRESEARCH |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 48.840, 71.670, 72.750 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 51.030 - 1.640 |
| R-factor | 0.206 |
| Rwork | 0.204 |
| R-free | 0.23700 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1c5m |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.251 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | MOLREP (V. 1) |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 1.710 |
| High resolution limit [Å] | 1.620 | 1.620 |
| Rmerge | 0.060 | 0.370 |
| Number of reflections | 32725 | |
| <I/σ(I)> | 15.5 | 4.33 |
| Completeness [%] | 98.7 | 97.1 |
| Redundancy | 5 | 4.77 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5.5 | pH 5.50 |
