2BKZ

STRUCTURE OF CDK2-CYCLIN A WITH PHA-404611

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-1
Synchrotron site	ESRF
Beamline	ID14-1
Temperature [K]	100
Detector technology	CCD
Collection date	2001-02-22
Detector	ADSC CCD
Spacegroup name	P 62 2 2
Unit cell lengths	183.862, 183.862, 214.572
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	29.800 - 2.600
Rwork	0.230
R-free	0.25900
Structure solution method	OTHER
RMSD bond length	0.006
RMSD bond angle	1.300
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	CNX (2002)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000	2.690
High resolution limit [Å]	2.600	2.600
Rmerge	0.080	0.530
Number of reflections	66033
<I/σ(I)>	18.2	3
Completeness [%]	99.7	99.8
Redundancy	4	4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		7		20% AMMONIUM SULPHATE, 1M KCL, 40MM HEPES PH 7